The Synthesis of New Solid-phase Microextraction Adsorption Material and Its Adsorption Performance

Shuang, Fu; Chunhui, Xia; Hongmei, Li; Feng, Xu

The Synthesis of New Solid-phase Microextraction Adsorption Material and Its Adsorption Performance

Fu Shuang^*, Xia Chunhui, Li Hongmei, Xu Feng

College of Pharmacy, Qiqihar Medical University, Heilongjiang, 161006, P.R. China

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Identifiers and Pagination:

Year: 2015
Volume: 9
First Page: 53
Last Page: 57
Publisher ID: TOCENGJ-9-53
DOI: 10.2174/1874123101509010053

Article History:

Received Date: 05/09/2013
Revision Received Date: 22/12/2013
Acceptance Date: 08/01/2014
Electronic publication date: 26/6/2015
Collection year: 2015

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© 2015 Shuang et al.

open-access license: This is an open access article distributed under the terms of the Creative Commons Attribution 4.0 International Public License (CC-BY 4.0), a copy of which is available at: https://creativecommons.org/licenses/by/4.0/legalcode. This license permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.

^* Address correspondence to this author at the College of Pharmacy, Qiqihar Medical University, Heilongjiang, 161006, P.R. China; Tel: 15846289920; E-mail: fsjt1980@163.com

This article uses three kinds of monomers: the styrene, butyl acrylate and Vinyltriisopropoxysilane, synthesized the solid phase micro extract coating adsorption material, carries on the structure characterization and the physical performance test. Takes it as the solid phase micro extract coating, carries on the inspection to its adsorbability, the experiment obtains the detection limit of the benzene which is 0.21 µ g/L; The detection limit of the toluene is 30 µ g/L; The detection limit of the m-Xylene is 0.55 µ g/L. Indicated the adsorptivity of this polymer has more effection toward the small molecular aromatic hydrocarbon as the solid phase micro extract coating adsorption material, and the limit of detection is lower compared to the commodity extract coating, there are some promotion and adoption value.

Keywords: Adsorptivity, solid phase micro extract coating, structure attribute.

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RESEARCH ARTICLE

The Synthesis of New Solid-phase Microextraction Adsorption Material and Its Adsorption Performance

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